Further information can be found in the documentation page . the possibility to calculate the radial distribution function. PASAD 2.0 contains a lot of additional features, e.g. by evaluating grain sizes using the peak broadening. This peak parameters can then be used for the quantitative local scale analysis e.g. Peak parameters are determined by fitting a combined model of all peaks using pseudo Voigt peak-functions. To ensure reproducibility the location of the splinepoints is determined automatically by detecting and prefitting the peaks. The background of the diffraction profile is subtracted using a spline fit. Furthermore elliptic distortions are corrected. As deviations from the correct center of integration can cause artificial peak broadening and even double peaks, the center is refined to sub-pixel pecission by the program. The PASAD-tools provide a Digital Micrograph™ Plugin with Graphical interface for full-automatic and fast determination of quantitative data from a SAD.įor quantitative analysis, the SAD have to be transformed in an electron diffraction profile by azimuthal integration. This is done by analysing parameters obtained using profile analysis of SAD (PASAD).
This is not possible using X-ray, but in the TEM quanitative analysis can be obtained from an electron diffraction pattern (SAD) taken from the area of interest. on grain and domain size or on the order parameter. When studying nanocrystalline materials, it is crucial to get quantitative information on a local scale, e.g.
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